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Recording exact reconstitution volumes, dates, storage conditions, and any observations supports reproducible results and proper experimental controls

The dual HPLC and mass-spec approach is the correct standard, since purity and identity are separate questions and a compound can be pure yet incorrectly identified

doi: 10.3389/fimmu.2023.1231047 199 KreideweissSSchanzleGSchnappGVintonyakVGrundlMA

Secondary plots of the k obs values from single exponential fits of the first phase and double exponential fits of the second phase against the GSSG concentration yielded a linear and hyperbolic correlation for the first and second phase, respectively (Fig

10.1016/j.mrgentox.2007.10.014 145